Bursa Uludağ Üniversitesi Açık Erişim Sistemi
Bursa Uludağ Üniversitesinin araştırma çıktılarının yer aldığı açık erişim sistemidir.
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http://hdl.handle.net/11452/22947| Başlık: | Synthesis of PbO nano-particles from a new one-dimensional lead(II) coordination polymer precursor |
| Yazarlar: | Sadeghzadeh, Homa Morsali, Ali Büyükgüngör, Orhan Uludağ Üniversitesi/Fen-Edebiyat Fakültesi/Kimya Bölümü. 0000-0002-2849-3332 Yılmaz, Veysel Turan L-7238-2018 7006269202 |
| Anahtar kelimeler: | Crystal structure Thermal properties Nano-materials Coordination reactions Diffraction Lead Lead oxide Materials properties Nanoparticles Scanning electron microscopy Surface active agents Thermodynamic stability X ray diffraction X ray powder diffraction Coordination environment Coordination polymers Elemental analysis IR spectroscopy Nano-materials Nano-scale materials One-dimensional coordination polymer Polymeric precursors Powder XRD Single crystal x-ray diffraction Thermal properties Thermal stability |
| Yayın Tarihi: | 15-Nis-2010 |
| Yayıncı: | Elsevier |
| Atıf: | Sadeghzadeh, H. vd. (2010). "Synthesis of PbO nano-particles from a new one-dimensional lead(II) coordination polymer precursor". Materials Letters, 64(7), 810-813. |
| Özet: | A new Pb(II) one-dimensional coordination polymer, [Pb(mu-NO2)(mu-pyc)(H2O)](n) (1). Hpyc = 2-pyridine-carboxylic acid] was prepared and characterized by elemental analyses, powder XRD diffraction and IR spectroscopy. Compound 1 was structurally characterized by single-crystal X-ray diffraction and one-dimensional coordination polymer with coordination environment of PbNO6. The thermal stability of compound 1 showed that compound 1 decomposes at 110-500 degrees C and the final product is PbO. This polymeric precursor has been used to make PbO nano-particles using two different surfactants. The new nano-structure was characterized by scanning electron microscopy and X-ray powder diffraction. This study demonstrates that the coordination polymers may be suitable precursors for the preparation of nanoscale materials. |
| URI: | https://doi.org/10.1016/j.matlet.2010.01.017 https://www.sciencedirect.com/science/article/pii/S0167577X10000297 http://hdl.handle.net/11452/22947 |
| ISSN: | 0167-577X 1873-4979 |
| Koleksiyonlarda Görünür: | Scopus Web of Science |
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